LYCOMING
COLLEGE
ADVANCED ANALYTICAL CHEMISTRY
CHEMISTRY
443, 1998
(Instrumental Analysis)
DESCRIPTION:
A study of instrumental analytical methods with emphasis on quantitative
applications of chromatographic,
electrochemical, and spectroscopic techniques.
CLASS HOURS: Lecture: MWF, 9:00 - 9:50 a.m.; Lab: T 1:00 - 4:50 p.m.
INSTRUCTOR: Dr. David A. Franz Office: 321-4181 Home: 326-7594 E-mail: franz@lycoming.edu
OFFICE HOURS: MWF, 11:15 - 12:00 a.m.; MF, 2:00 - 3:00 p.m.; or by appointment
TEXT:
Harris, D. C. Quantitative Chemical Analysis, 4th Ed.; Freeman:
New York, 1995. Readings from other texts
and sources will also be made.
LAB POLICIES:
Safety glasses and bound lab notebook required; no bare feet, sandals or
shorts in lab. Written lab reports
will be due one week following completion of each experiment. Late reports
will be docked five points plus
one point per day late.
EXAMS:
There will be three exams and a comprehensive final (ACS Standardized).
Exam dates:
February 03, Tuesday lab period
March 10, Tuesday lab period
April 07, Tuesday lab period
HOMEWORK: Will be assigned regularly, collected and checked.
GRADING
SCHEME: Exams
300
Extra Credit: 3 pts added for each
Final
100
Chem Colloquium attended, in excess
Lab Experiments 300
of class absences. Class absences:
Class, HW
100
3 pts @ deducted in excess of 3 absences.
TOTAL 800
Letter
grades will be assigned on the following basis:
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| Week | General Topic | Chapter | Laboratory | |
| 1 | Jan 05 | Fundamentals of Electrochemistry | 14 | Check-in |
| 2 | Jan 12 | Potentiometry & ISE's; Electrodepositions | 15, 17 | 1. Pot. Titr. & Nernst Eqn. |
| 3 | Jan 19 | Coulometry; Voltammetry & Polarography | 17, 18 | 2. Voltammetry |
| 4 | Jan 26 | Voltammetry: advanced techniques | 18 | 3. ISE's |
| 5 | Feb 02 | Separation Theory | 22 | EXAM I |
| 6 | Feb 09 | Gas Chromatography (GC) | 23 | 4. GC using Int Std |
| 7 | Feb 16 | High Performance Liquid Chrom. (HPLC) | 23 | 5. HPLC - computer simulations |
| Feb 23 SPRING BREAK | ||||
| 8 | Mar 02 | Capillary Electrophoresis (CE and CIA) | 24 | 6. HPLC - lab exp |
| 9 | Mar 09 | Mass Spectrometry (MS and GC-MS) | - | EXAM II |
| 10 | Mar 16 | Spectrophotometry; UV-VIS | 6, 19 | 7. GC-MS Exam II |
| 11 | Mar 23 | Fluorescence; Spectrophotometers | 19, 20 | 8. FTIR or UV-VIS |
| 12 | Mar 30 | Atomic Spectroscopy (AA/FE) | 21 | 9. AA using Std Addns |
| 13 | Apr 06 | IR and Fourier Transform IR (FTIR) | 20 | EXAM III; Check-out |
| 14 | Apr 13 | Evals; Thermal Methods; Applied Problems | - | Field Trip to Merck |
| 15 | Apr 20 | Final Exams |
Last updated January 7, 1998.
The URL for this page is
http://lyco2.lycoming.edu/dept/chem/spring1998/syl443.htm