every effort has been made to make sure this electronic syllabus is error-free,
it is not official.
The definitive source of course information remains the original (paper) syllabus distributed in class.
ADVANCED ANALYTICAL CHEMISTRY
A study of instrumental analytical methods with emphasis on
quantitative applications of chromatographic, electrochemical, and
Lecture: MWF, 11:30 - 12:20 a.m.;
Lab: T 1:00 - 4:50 p.m.
Dr. David A. Franz Office:
321-4181 Home: 326-7594
MWF, 9:30 - 11:00 a.m.; WF,
1:00 - 2:00 p.m.; or by
Harris, D. C. Quantitative Chemical Analysis, 5th Ed.; Freeman: New York, 1999.
Readings from other texts and sources will also be made.
Safety glasses and bound lab notebook required; no bare feet, sandals
or shorts in lab. Carbons of lab
data are due at the end of the day work is done.
Written lab reports will be due one week following completion of each
experiment, or as announced. Late
reports will be docked five points plus one point per day late.
There will be two exams, a shorter take-home exam, and a comprehensive
final (ACS Standardized). Exam
dates (subject to change by unanimous consent):
February 12, Tuesday lab period
March 26, Tuesday lab period
Will be assigned regularly, collected and checked.
3 pts @ deducted in excess of 3 absences.
Letter grades will be assigned on the following basis:
100-91% = A
90-89% = A-
|1||Jan 07||Separation Theory||23||1. GC using Int. Std.|
|2||Jan 14||Gas Chromatography (GC)||24||2. HPLC - computer intro.|
|3||Jan 21||High Performance Liquid Chrom. (HPLC)||25||Field Trip|
|4||Jan 28||Capillary Electrophoresis (CE and CIA)||26||3. HPLC - lab exp|
|5||Feb 04||Mass Spectrometry (MS and GC-MS)||24||4. GC-MS|
|6||Feb 11||Sample Clean-up (SPE and SPME)||14||EXAM I|
|7||Feb 18||Fundamentals of Electrochemistry||15||5. I-/Cl- & Nernst Eqn.|
|Feb 25||SPRING BREAK|
|8||Mar 04||Potentiometry & Ion Selective Electrodes (ISE's)||17||6. ISE's|
|9||Mar 11||Voltammetry & Polarography||18||7. Voltammetry|
|10||Mar 18||Voltammetry: advanced techniques||19||Field Trip|
|11||Mar 25||Spectrophotometry; UV-VIS||20, 21||EXAM II|
|12||Apr 01||Fluorescence; Spectrophotometers||22||8. AA Using Std. Addns|
|13||Apr 08||Atomic Spect. (AA/FE); IR and FTIR||21||Check-out|
|14||Apr 15||Evals; Thermal Methods; Applied Problems||-||Field Trip|
|15||Apr 22||Final Exams|
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